Refinement of lithium tetrahydroxoborate with low-temperature CCD data

Authors
Fronczek, FR Aubry, DA Stanley, GG
Citation
Fr. Fronczek et al., Refinement of lithium tetrahydroxoborate with low-temperature CCD data, ACT CRYST E, 57, 2001, pp. I62-I63
Citations number
9
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
ISSN journal
16005368 → ACNP
Volume
57
Year of publication
2001
Part
8
Pages
I62 - I63
Database
ISI
SICI code
1600-5368(200108)57:<I62:ROLTWL>2.0.ZU;2-1
Abstract
Refinement of the title compound, Li B(OH)(4), with CCD data at 120 K has l ed to a sevenfold increase in precision over the previously reported struct ure based on film data. The H atoms have been located and refined. Both Li and B are tetrahedrally coordinated. B-O distances are in the range 1.4644 (14)-1.4989 (13) A E, while LiDO distances are in the range 1.931 (2)-2.022 (2) Angstrom.