Resolution of 8 '-alkoxy- and hydroxy-1,1 '-binaphthalen-8-ols

Authors
Hua, DH Nguyen, TXC McGill, JW Chen, Y Robinson, PD
Citation
Dh. Hua et al., Resolution of 8 '-alkoxy- and hydroxy-1,1 '-binaphthalen-8-ols, TETRAHEDR-A, 12(14), 2001, pp. 1999-2004
Citations number
14
Categorie Soggetti
Organic Chemistry/Polymer Science
Journal title
TETRAHEDRON-ASYMMETRY
ISSN journal
09574166 → ACNP
Volume
12
Issue
14
Year of publication
2001
Pages
1999 - 2004
Database
ISI
SICI code
0957-4166(20010814)12:14<1999:RO8'AH>2.0.ZU;2-U
Abstract
Enantiopure 8 ' -ethoxy-, 8 ' -hydroxy-, and 8 ' -methoxy-1,1 ' -binaphthal en-8-ol were readily resolved by separating the corresponding chiral campha nic esters [derived from the esterification of the alcohols with (-)-(1S)-c amphanie chloride] based upon their differing solubility in diethyl ether a nd their differing chromatographic behavior. (C) 2001 Elsevier Science Ltd. All rights reserved.