Dehydration of sodium carbonate decahydrate to monohydrate in a fluidized bed

Citation
M. Hartman et al., Dehydration of sodium carbonate decahydrate to monohydrate in a fluidized bed, AICHE J, 47(10), 2001, pp. 2333-2340
Citations number
30
Categorie Soggetti
Chemical Engineering
Journal title
AICHE JOURNAL
ISSN journal
00011541 → ACNP
Volume
47
Issue
10
Year of publication
2001
Pages
2333 - 2340
Database
ISI
SICI code
0001-1541(200110)47:10<2333:DOSCDT>2.0.ZU;2-2
Abstract
Kinetics of the thermal dehydration of sodium carbonate decahydrate to mono hydrate is investigated at temperatures between 15 and 30 degreesC in a bat ch, fluidized-bed, 140-mm-ID reactor. Effects of particle size, mass of bed , and gas velocity on the dehydration rate are also explored. A simple corr elation based on the collected experimental data is developed. The proposed rate law formula makes it possible to estimate the dehydration rate that w ould be needed to design the performance of a fluidized-bed drying unit. Th e produced monohydrate is subjected to textural analysis, and pore volume a nd surface-area data are presented.