Gq. Xie et al., Effect of interface behavior between particles on properties of pure Al powder compacts by spark plasma sintering, MATER TRANS, 42(9), 2001, pp. 1846-1849
Pure Al powder was sintered by spark plasma sintering (SPS) process at vari
ous sintering temperatures and loading pressures. The density, electrical r
esistivity, tensile properties and microstructure of powder compacts were i
nvestigated, The powder compacts with the similar properties as base alumin
um metal was obtained at sintering temperature above 873 K, loading pressur
e above 23.5 MPa. For the powder compacts with the similar density but with
the large difference in the electrical resistivity and tensile properties,
the interfaces between Al powder particles were investigated using high re
solution transmission electron microscopy (HRTEM) and energy dispersive X-r
ay spectroscopy (EDS). Two types of interfaces, with metal/metal bonding an
d metal/oxide film layer/metal bonding, were observed in Al powder compacts
. The properties of powder compacts were mainly subject to the behavior of
oxide film between the powder particles.