Hydrodynamics and scale-up of horizontal stirred reactors

Citation
Gjs. Van Der Gulik et al., Hydrodynamics and scale-up of horizontal stirred reactors, IND ENG RES, 40(22), 2001, pp. 4731-4740
Citations number
24
Categorie Soggetti
Chemical Engineering
Journal title
INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
ISSN journal
08885885 → ACNP
Volume
40
Issue
22
Year of publication
2001
Pages
4731 - 4740
Database
ISI
SICI code
0888-5885(20011031)40:22<4731:HASOHS>2.0.ZU;2-G
Abstract
In this study, the hydrodynamics in horizontal stirred-tank reactors are in vestigated. The flow state, agitation power, and macromixing time have been determined experimentally. Two flow states, i.e., "slosh" and "ring", can be distinguished, with transition between the two states that shows hystere sis. The agitation power was determined by measuring the temperature increa se upon mixing. The power number appears to be comparable to power numbers in unbaffled vertical vessels. A variation in fill ratio indicates that agi tation energy dissipates uniformly throughout the reactor under laminar con ditions. Under turbulent conditions, however, most energy is dissipated at the vessel wall. Using pulse-response measurements, macromixing times have been determined. The mixing times correlate with momentum input and liquid volume, thus indicating different hydrodynamics at large and small scales. A combination of mixing,, times and agitation power shows that, at small sc ale and intermediate fill ratios, the mixing is most energy-efficient.