Synthesis, structure, and characterization of polymeric stationary phase derived from (R,R)-tartramide and bisphenol-S

Authors
Jablonska-Pikus, T Charmas, W Podkoscielna, B Gawdzik, B
Citation
T. Jablonska-pikus et al., Synthesis, structure, and characterization of polymeric stationary phase derived from (R,R)-tartramide and bisphenol-S, J APPL POLY, 82(14), 2001, pp. 3409-3417
Citations number
12
Categorie Soggetti
Organic Chemistry/Polymer Science","Material Science & Engineering
Journal title
JOURNAL OF APPLIED POLYMER SCIENCE
ISSN journal
00218995 → ACNP
Volume
82
Issue
14
Year of publication
2001
Pages
3409 - 3417
Database
ISI
SICI code
0021-8995(200112)82:14<3409:SSACOP>2.0.ZU;2-X
Abstract
The preparation of a new chiral polymeric stationary phase for chromatograp hy is presented. A porous copolymer of mono- and dimethacrylate derivatives of bisplienol-S and divinylbenzene containing hydroxyl functional groups w as used as a matrix. (3-Aminopropyl)triethoxysilane was used as a coupling agent and was bonded to these groups. The obtained compound was transferred into a final product during a three-step synthesis. The properties of the obtained polymeric phase with the chiral moiety were studied. (C) 2001 John Wiley & Sons, Inc.