T. Sekino et K. Niihara, FABRICATION AND MECHANICAL-PROPERTIES OF FINE-TUNGSTEN-DISPERSED ALUMINA-BASED COMPOSITES, Journal of Materials Science, 32(15), 1997, pp. 3943-3949
The mechanical properties and microstructure of fine-tungsten-disperse
d alumina-based composites, which were fabricated by hot pressing a mi
xture of fine alpha-Al2O3 and W powders, have been investigated. Small
W particles of approximately 140 nm average size were located within
the Al2O3 matrix grains. The mechanical properties were influenced by
the metal content and sintering conditions. When the appropriate W con
tent and sintering condition were selected (typically 5-10 vol% W and
sintered at 1400 degrees C), the fracture strength was enhanced compar
ed with that of monolithic Al2O3. The metal content dependence of Youn
g's modulus and the Vickers hardness did not obey the rule of mixtures
. This may be attributed to the presence of localized residual stress
caused by the incorporation of fine W dispersion into Al2O3. On the ot
her hand, high-temperature (1600 degrees C) sintering caused degradati
on in the properties of the composites due to the grain growth and che
mical reaction of W dispersion, which was revealed by X-ray photoelect
ron spectroscopy analysis. The relations between fabrication condition
and mechanical properties are discussed.