S. Ozbilen, FRACTOGRAPHY AND TRANSMISSION ELECTRON-MICROSCOPY ANALYSIS OF AN AL-LI-CU-MG-ZR ALLOY DISPLAYING AN IMPROVED FRACTURE-TOUGHNESS, Journal of Materials Science, 32(15), 1997, pp. 4127-4131
Al-2.3 wt % Li-1.8 wt % Mg-0.15 wt % Zr alloys with 0.1 and 0.45 wt %
Cu were studied. The materials were cast, homogenized at 530 degrees C
for 24 h, extruded at 400 degrees C with a reduction ratio of 30 : 1,
solution treated at 528 degrees C for 0.5 h and then artificially age
d at 190 degrees C to an overaged condition. The concerted application
of light-, transmission electron- and scanning electron microscopy to
gether with short rod fracture toughness measurements allowed the infl
uence of low level Cu together with 0.15 wt % Zr on the fracture tough
ness of this alloy system to be studied. It was found that the additi
on of 0.1 wt % Cu together with 0.15 wt % Zr not only affected the del
ta' precipitate nucleation and their size and size distribution throug
h Li-Cu-v triple complexes but also affected the beta' dispersoid nucl
eation through Zr-Cu-v triple complexes. This in turn affected the siz
e and size distribution of the delta'/beta' duplex precipitates. This
causes an increase in the fracture toughness in underaged material art
ificially aged at 190 degrees C. This effect was probed in an SEM frac
tographic investigation and by mechanical testing.