The adhesion between electrolessly-deposited copper and photosensitive epox
y was measured with a pull test designed in this work. The test pads were f
abricated on the epoxy substrate using a semi-additive plating process. The
pull strength was measured with a mechanical tester. A chemical treatment
was used to roughen the epoxy surface; two sets of specimens were tested wi
th different swelling and etching times to obtain the optimal adhesion stre
ngth. Another set of specimens was tested as reference without swelling. Th
e effects of the chemical treatment on surface topography and adhesion were
studied. The surface topography of the epoxy was examined by optical micro
scopy, scanning electron microscopy (SEM), and energy-dispersive spectrosco
py (EDS). The ranges of swelling and etching times, which resulted in good
adhesion, were presented. It was confirmed that the procedure of swelling a
nd etching processes had to be optimized for achieving the desired epoxy su
rface properties without altering the bulk properties.