Synthesis of crown ethers based on 9,9-bis-(4-hydroxyphenyl)fluorene and structural determination by X-ray single crystallography

Authors
Lee, KJ Park, J Park, JW Koo, SM
Citation
Kj. Lee et al., Synthesis of crown ethers based on 9,9-bis-(4-hydroxyphenyl)fluorene and structural determination by X-ray single crystallography, B KOR CHEM, 22(10), 2001, pp. 1101-1104
Citations number
17
Categorie Soggetti
Chemistry
Journal title
BULLETIN OF THE KOREAN CHEMICAL SOCIETY
ISSN journal
02532964 → ACNP
Volume
22
Issue
10
Year of publication
2001
Pages
1101 - 1104
Database
ISI
SICI code
0253-2964(20011020)22:10<1101:SOCEBO>2.0.ZU;2-6
Abstract
We report the synthesis and characterization of [38], [57], [76] and [48]-m embered crown ethers including bis-(hydroxyphenyl)fluorene in the macroring . Four crown ethers 1-4 are characterized by MALDI-mass spectral data and H -1-NMR data. Also, structural determination of [38]-membered crown ether 1 has been performed by X-ray crystallography.