H. Plaisantin et al., Conversion of cellulosic fibres into carbon fibres: a study of the mechanical properties and correlation with chemical structure, COMP SCI T, 61(14), 2001, pp. 2063-2068
Rayon fibres were pyrolysed under inert gas flows up to 1200 degreesC. Chan
ges in the mechanical properties of the fibres at various stages of the the
rmal treatment were studied and correlated with structural analyses of the
char by CP/MAS C-13 NMR and DRIFT spectroscopies. The force/displacement cu
rve of fibres pyrolysed at 500 degreesC is non-linear but reversible within
the deformation, which is approximately 10% at ultimate failure. (C) 2001
Elsevier Science Ltd. All rights reserved.