Dj. Barnard et al., ACOUSTIC HARMONIC-GENERATION DUE TO THERMAL EMBRITTLEMENT OF INCONEL-718, Journal of nondestructive evaluation, 16(2), 1997, pp. 67-75
This paper describes an attempt to characterize the deterioration of a
structural material's mechanical properties by nonlinear acoustics. I
n this particular case, the damage was caused by ''thermal embrittleme
nt'' during which the material, here the nickel-based alloy Inconel 71
8, loses a significant fraction of its fracture toughness. Harmonic ge
neration was the experimental method used to characterize the microstr
uctural changes in the material as a function of exposure time at elev
ated temperatures. Tests were performed on two heats of Inconel 718 wi
th slightly different chemistries, with one heat showing particular se
nsitivity of the fracture toughness to the elevated temperature exposu
re with corresponding higher changes in the nonlinearity parameter. As
a mechanical measure of the fracture toughness deterioration, a small
specimen punch test was used in which the ductility of a thin slice o
f material is determined. A clear difference between the two heats was
noted in the metallographic examination, which is reflected in the ha
rmonic generation as well as the punch test data. An explanation for t
he changes of the harmonic generation during the embrittlement process
is speculative at the present time.