Green state joining of SiC without applied pressure

Authors
Citation
J. Zheng et M. Akinc, Green state joining of SiC without applied pressure, J AM CERAM, 84(11), 2001, pp. 2479-2483
Citations number
17
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
JOURNAL OF THE AMERICAN CERAMIC SOCIETY
ISSN journal
00027820 → ACNP
Volume
84
Issue
11
Year of publication
2001
Pages
2479 - 2483
Database
ISI
SICI code
0002-7820(200111)84:11<2479:GSJOSW>2.0.ZU;2-X
Abstract
External pressure (uniaxial or isostatic) is usually necessary to form a th in and defect-free joint in green state joining of Sic ceramics. A successf ul method of joining Sic in the green state using a liquid polymer precurso r, allylhydridopolycarbosilane (AHPCS), without applied pressure, is descri bed. The thermal decomposition behavior of the polymer was examined, and de fect formation during joint evolution was investigated by interrupting the heat treatment at various stages. Cracks and pores were observed in the joi nts formed by pure AHPCS during the pyrolysis of the polymer precursor. Add ing Sic powder to the joining paste eliminated defect formation. Optimum Si c loading in the paste was determined to be in the range of 25-35 vol%. Joi nts formed by AHPCS + (SiC + 5 wt% B) paste were essentially indistinguisha ble from the matrix and had an average strength of 323 MPa, comparable to t hat of the control sample.