Micro-coiled carbon fibers were prepared by catalytic pyrolysis of acetylen
e with nanosized nickel powder catalyst using the substrate method. The mor
phology of micro-coiled carbon fibers was observed through field emission s
canning electron microscopy. It was found that the fiber and coil diameter
of the obtained micro-coiled carbon fibers is about 500-600 nm and 4-5 mum,
respectively. Most of the micro-coiled carbon fibers obtained were regular
double carbon coils, but a few irregular ones were also observed. On the b
asis of the experimental observation, a solid catalytic growth mechanism of
micro-coiled carbon fibers was proposed.