Arrays of Fe1-xNix(0 < x less than or equal to 0.32) alloys nanowires with
16nm in diameter and 4 mum in length have been successfully fabricated by e
lectrochemical method in anodic alumina oxide template. In the region of lo
w concentration Ni (0 < x less than or equal to 0.32), the structures of al
loy nanowires are all bcc structure with a preferred crystallographic orien
tation [110]. Mossbauer study shows that the direction of the moments of ir
on atoms in the nanowire is parallel to the axis of the nanowire, and the h
yperfine field of the sites of iron atoms has a little variation with incre
asing Ni content, which is consistent with the bulk Fe1-xNix alloy.