Synthesis of monosilane by catalytic disproportionation of trichlorosilanein a reaction-rectification apparatus with recycle

Authors
Vorotyntsev, VM Mochalov, GM Nipruk, OV
Citation
Vm. Vorotyntsev et al., Synthesis of monosilane by catalytic disproportionation of trichlorosilanein a reaction-rectification apparatus with recycle, RUS J AP CH, 74(4), 2001, pp. 621-625
Citations number
13
Categorie Soggetti
Chemistry
Journal title
RUSSIAN JOURNAL OF APPLIED CHEMISTRY
ISSN journal
10704272 → ACNP
Volume
74
Issue
4
Year of publication
2001
Pages
621 - 625
Database
ISI
SICI code
1070-4272(200104)74:4<621:SOMBCD>2.0.ZU;2-E
Abstract
Basic principles of a procedure for calculating a reaction-rectification ap paratus for synthesizing silane by catalytic disproportionation of trichlor osilane are presented. Technological parameters are substantiated and the p rocess of silane synthesis in the reaction-rectification apparatus is optim ized.