Pj. Hurley et Pd. Hodgson, Effect of process variables on formation of dynamic strain induced ultrafine ferrite during hot torsion testing, MATER SCI T, 17(11), 2001, pp. 1360-1368
Ultrafine grain sizes were produced using hot torsion testing of a 0.11C-1.
68Mn-0.20Si (wt-%) steel, with ultrafine ferrite (< 1 mum) nucleating intra
granularly during testing by dynamic strain induced transformation. A syste
matic study was made of the effect of isothermal deformation temperature, s
train level, strain rate, and accelerated cooling during deformation on the
formation of ultrafine ferrite by this process. Decreasing the isothermal
testing temperature below the Ae(3) temperature led to a greater driving fo
rce for ferrite nucleation and thus more extensive nucleation during testin
g; the formation of Widmanstatten ferrite prior to, or early during, deform
ation imposed a lower temperature limit. Increasing the strain above that w
here ferrite first began (0.8 at 675 C and a strain rate of 3 s(-1)) increa
sed the intragranular nucleation of ferrite. Strain rate appeared to have l
ittle effect on the amount of ferrite formed. However, slower strain rates
led to extensive polygonisation of the ferrite formed because more time was
available for ferrite recovery. Accelerated cooling during deformation fol
lowed by air cooling to room temperature led to a uniform microstructure co
nsisting of very fine ferrite grains and fine spherical carbides located in
the grain boundaries regions. Air cooling after isothermal testing led to
carbide bands and a larger ferrite grain size.