Solvent-free preparation of ionic liquids using a household microwave oven

Citation
Rs. Varma et Vv. Namboodiri, Solvent-free preparation of ionic liquids using a household microwave oven, PUR A CHEM, 73(8), 2001, pp. 1309-1313
Citations number
17
Categorie Soggetti
Chemistry
Journal title
PURE AND APPLIED CHEMISTRY
ISSN journal
00334545 → ACNP
Volume
73
Issue
8
Year of publication
2001
Pages
1309 - 1313
Database
ISI
SICI code
0033-4545(200108)73:8<1309:SPOILU>2.0.ZU;2-L
Abstract
An efficient solventless protocol for the preparation of a wide variety of ionic liquids is described, which requires a simple exposure of admixed 1-m ethylimidazole and alkyl halides to microwave irradiation in open glass con tainers. The details of this clean process using a common household microwa ve oven, which exploits the newer inverter technology system for better pow er attenuation, are described. The characterization and thermal stability d ata on selected ionic liquids and their potential applications are summariz ed.