A torsional rheometer with a double slit arrangement suitable for fast gelation

Citation
M. Lechtenfeld et al., A torsional rheometer with a double slit arrangement suitable for fast gelation, RHEOL ACT, 40(6), 2001, pp. 533-537
Citations number
13
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
RHEOLOGICA ACTA
ISSN journal
00354511 → ACNP
Volume
40
Issue
6
Year of publication
2001
Pages
533 - 537
Database
ISI
SICI code
0035-4511(200111)40:6<533:ATRWAD>2.0.ZU;2-9
Abstract
A home built torsional rheometer is presented that consists of a measuring cell with a double slit arrangement. This double slit arrangement guarantee s a quick cooling down of the sample which is of major importance for the o bservation of the start of the solgel transition under isothermal condition s. This torsional rheometer is based on an earlier version of a home built dynamic viscometer. The modifications are focusing first and foremost on th e miniaturizing of the measuring cell. This results in high cooling rates, small volume of the sample, small weight of the oscillating cylinder, and t herefore a relatively large range of frequencies.