Determination of biogenic amines in wine by multidimensional liquid chromatography with online derivatisation

Citation
T. Hyotylainen et al., Determination of biogenic amines in wine by multidimensional liquid chromatography with online derivatisation, ANALYST, 126(12), 2001, pp. 2124-2127
Citations number
15
Categorie Soggetti
Chemistry & Analysis","Spectroscopy /Instrumentation/Analytical Sciences
Journal title
ANALYST
ISSN journal
00032654 → ACNP
Volume
126
Issue
12
Year of publication
2001
Pages
2124 - 2127
Database
ISI
SICI code
0003-2654(2001)126:12<2124:DOBAIW>2.0.ZU;2-0
Abstract
An online multidimensional liquid chromatographic system was developed for online clean-up, derivatisation and separation of biogenic amines in wines. The system consists of a cation-exchange precolumn, a derivatisation coil and an analytical column, and a column-switching valve. The entire system c an be easily automated. The method proved to be quantitative and sensitive. Limits of detection were below 0.05 mg l(-1) for all amines and linearity was preserved over the tested range (0.05-15 mg l(-1)). The method was appl ied to the analysis of red wines of different origin.