Polymeric nanocomposites were prepared by direct mixing of ultrafine diamon
ds with a PC melt, The structural and mechanical properties of the composit
es were studied by small-angle X-ray scattering (SAXS) and tensile test tec
hniques. The mixing process is accompanied by changes in the basic paramete
r of fractal structure of ultrafine diamond powders and their intense deagg
regation, which results in a sharp increase in the proportion of SAXS-detec
table particles. The subsequent self-assembling of disintegrated particles
into an infinite percolation cluster leads to a significant decline in the
deformation properties of the composite even at small concentrations.