In this letter, we show that normal-incidence spectroscopic ellipsometry ca
n be used for high-accuracy topography measurements on surface relief grati
ngs. We present both experimental and theoretical results which show that s
pectroscopic ellipsometry or reflectance-difference spectroscopy at near-no
rmal incidence coupled with vector diffraction theory for data analysis is
capable of high-accuracy critical dimension (CD), feature height, and sidew
all angle measurements in the extreme submicron regime. Quantitative compar
isons of optical and cross-sectional scanning electron microscopy (SEM) top
ography measurements from a number of 350 nm line/space reactive-ion-etched
Si gratings demonstrate the strong potential for in situ etching monitorin
g. This technique can be used for both ex situ and in situ applications and
has the potential to replace the use of CD-SEM measurements in some applic
ations. (C) 2001 American Institute of Physics.