Atomic force microscopy is applied for investigation of amorphous silicon a
nd zirconium oxide insulator (a-Si/ZrOx) or amorphous germanium (a-Si/a-Ge)
multilayer nanostructures (MNS) prepared by electron beam evaporation. Per
iodicity of a-Si/ZrOx MNS has been confirmed by Auger-spectroscopy. The etc
hing wedge profile of a-Si/ZrOx MNS shows a series of terraces and steps wh
ose number corresponds to the number of periods of the MNS. The MNS period
determined by this method agree with that obtained by small angle X-ray dif
fraction. At the cross-section of a-Si/a-Ge MNS the a-Si and a-Ge single-la
yers are resolved.