Sonochemical synthesis of nanophase indium sulfide

Citation
S. Avivi et al., Sonochemical synthesis of nanophase indium sulfide, CHEM MATER, 13(6), 2001, pp. 2195-2200
Citations number
32
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
CHEMISTRY OF MATERIALS
ISSN journal
08974756 → ACNP
Volume
13
Issue
6
Year of publication
2001
Pages
2195 - 2200
Database
ISI
SICI code
0897-4756(200106)13:6<2195:SSONIS>2.0.ZU;2-U
Abstract
The sonication of InCl3 with thioacetamide in an aqueous solution has led t o different products, depending on the sonication temperature. Sonication a t 0 degreesC yielded In2O3 as the major product and In2S3 as a minor compon ent. On the other hand, when the reaction is carried out at "room temperatu re", nanocrystalline In2S3 is obtained as the sole product. The products of sonication at 0 degreesC are obtained in the amorphous form. An explanatio n for this is offered based on the hot spot mechanism.