J. Solymosi et al., DETERMINATION OF RADIOACTIVE BULK AND SURFACE CONCENTRATION BY BETA-DETECTION .3. CORRECTION FOR GAMMA-BACKGROUND, Journal of radioanalytical and nuclear chemistry, 209(1), 1996, pp. 27-39
A method for determining bulk or surface activity concentration of bet
a-emitters in ''infinitely'' thick or thin samples using energy select
ive detectors without any prior chemical separation or qualitative ana
lysis was introduced in Part I. In addition to that method, a correcti
on procedure is often required in order to compensate for the gamma-se
nsitivity of the beta-detector. A system or two - preferably identical
- detectors positioned to the front and rear side of a sample has bee
n established. The rear side detector is shielded against beta-radiati
on. The gamma-response of both detectors is determined as a function o
f gamma-energy using monoenergetic calibration standards. Response pul
ses are selected to form 8 or 16 energy intervals, and separate series
of correction coefficients are then computed for each interval and st
andard energy using the ratio of the respective counts. When a sample
having mixed beta- and gamma-radiation is evaluated, an ''effective''
gamma-energy is first calculated from the pulse height distribution of
the rear side detector, the appropriate series of correction coeffici
ents is selected and finally net beta-counts are generated from the co
unts of the front side detector. Sensitivities in natural and elevated
gamma-background are presented.