Some analytical techniques are able to produce images, making if possible t
o obtain a large amount of information. Working with images, the pixels can
be treated like objects in a data matrix. In this way, a multi-way PCA of
micrograph images was applied to the internal surface of a Teflon coil used
for microwave sample digestion. This Teflon coil was used for 120h and had
been attacked with different acids. It was cut into 3 pieces (namely: init
ial, medium and central portions) in order to obtain 7 micrographs (2 for i
nitial, 2 for medium and 3 for the central part). A micrograph of a piece f
rom a new Teflon coil was used for comparison. With these 8 micrographs, it
was possible to establish a three-dimensional arrangement. After multi-way
PCA was applied to the Teflon surface images, was possible to group a grea
t amount of information and to characterise different parts of this coil.