DETERMINATION OF THE RODENTICIDES WARFARIN, DIPHENADIONE AND CHLOROPHACINONE IN SOIL SAMPLES BY HPLC-DAD

Authors
MEDVEDOVICI A DAVID F SANDRA P
Citation
A. Medvedovici et al., DETERMINATION OF THE RODENTICIDES WARFARIN, DIPHENADIONE AND CHLOROPHACINONE IN SOIL SAMPLES BY HPLC-DAD, Talanta, 44(9), 1997, pp. 1633-1640
Citations number
26
Journal title
Talanta
ISSN journal
00399140 → ACNP
Volume
44
Issue
9
Year of publication
1997
Pages
1633 - 1640
Database
ISI
SICI code
0039-9140(1997)44:9<1633:DOTRWD>2.0.ZU;2-N
Abstract
A HPLC-DAD method is described for the analysis of the rodenticides wa rfarin, diphenadione and chlorophacinone, together with the phenylurea herbicides isoproturon and diuron, in soil samples. The HPLC paramete rs have been optimised to provide baseline separation with symmetrical peakshapes in short analysis times. The sample preparation consists o f Soxhlet extraction followed by SPE clean-up on cyanopropyl silica. ( C) 1997 Elsevier Science B.V.