Barium ferrite powders obtained by co-precipitation

Citation
Sr. Janasi et al., Barium ferrite powders obtained by co-precipitation, PHYS ST S-A, 185(2), 2001, pp. 479-485
Citations number
8
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
PHYSICA STATUS SOLIDI A-APPLIED RESEARCH
ISSN journal
00318965 → ACNP
Volume
185
Issue
2
Year of publication
2001
Pages
479 - 485
Database
ISI
SICI code
0031-8965(20010616)185:2<479:BFPOBC>2.0.ZU;2-9
Abstract
Barium ferrites are usually produced by the ceramic method. On the other ha nd, very fine particles with high chemical homogeneity can be obtained by w et methods, such as co-precipitation, In this work, barium ferrite powders were obtained by co-precipitation. The effects of Fe/Ba molar ratio, reagen t addition order, pH, temperature calcination and the presence of NaCl duri ng calcination were investigated. The products were characterized by differ ential thermal analysis, X-ray diffractometry and scanning electron microsc opy. The magnetic properties were evaluated by a vibrating sample magnetome ter. The presence of a large amount of NaCl during calcination had a detrim ental effect on the magnetic properties. Very fine particles with intrinsic coercivities up to 440 kA/m (5.50 kOe) and saturation magnetization sigma (s) up to 71 Am-2/kg (71 emu/g) were achieved.