A new scanning transmission electron microscope has been developed for thre
e-dimensional (3D) observations of nanostructures. Using double spherical f
ulcra, accurate eucentric rotation was achieved. Cylindrical specimens for
3D-observation were prepared by a microsampling technique using a focused i
on beam. Copper via-holes of a semiconductor memory device and ZnO particle
s were observed by the 3D-STEM from different directions, and 3D-data of th
e ZnO particles were successfully reconstructed in a topography mode.