Xl. Tan et al., In situ transmission electron microscopy observations of electric-field-induced domain switching and microcracking in ferroelectric ceramics, MAT SCI E A, 314(1-2), 2001, pp. 157-161
In situ transmission electron microscopy (TEM) technique was developed to e
xamine micromechanisms of the electric fatigue in ferroelectric ceramics. T
he technique was based on a specially designed specimen connected to a modi
fied TEM heating stage. With this technique, domain switching and nanodomai
n alignment near crack-like flaws were observed under cyclic electric field
s. Following repeated electric cycles. microcracks were found to develop al
ong domain and grain boundaries. (C) 2001 Elsevier Science B,V. All rights
reserved.