The extraction and cromatographic analysis of some aromatic gritstone compounds of creosote type

Citation
J. Carre et al., The extraction and cromatographic analysis of some aromatic gritstone compounds of creosote type, REV RO CHIM, 46(1), 2001, pp. 31-34
Citations number
15
Categorie Soggetti
Chemistry
Journal title
REVUE ROUMAINE DE CHIMIE
ISSN journal
00353930 → ACNP
Volume
46
Issue
1
Year of publication
2001
Pages
31 - 34
Database
ISI
SICI code
0035-3930(200101)46:1<31:TEACAO>2.0.ZU;2-X
Abstract
This paper studied the possibility of extraction and analysis of eleven org anic compounds of creosote type from gritstone, the representative material of the area under study from Great Britain (polluted and abandoned). The e xtraction was made with a mixture of dichloromethane: acetone, by cryogenic grinding, while the analysis was made by GC/FID and GC/MS. Three levels of pollution were tested for each pollutant, 0.2; 1.0 and 10 ppm. The average extraction output was of 90% while the average CV was of 10%. The analysis lasted for two hours.