THE PREPARATION, SPECTRAL AND X-RAY CRYSTALLOGRAPHIC CHARACTERIZATIONOF 2,6-DIACETYLPYRIDINEDIHYDRAZONE COMPLEX WITH LEAD(II)NITRATE

Authors
RADECKAPARYZEK W GDANIEC M
Citation
W. Radeckaparyzek et M. Gdaniec, THE PREPARATION, SPECTRAL AND X-RAY CRYSTALLOGRAPHIC CHARACTERIZATIONOF 2,6-DIACETYLPYRIDINEDIHYDRAZONE COMPLEX WITH LEAD(II)NITRATE, Polyhedron, 16(20), 1997, pp. 3681-3686
Citations number
37
Categorie Soggetti
Chemistry Inorganic & Nuclear",Crystallography
Journal title
Polyhedron → ACNP
ISSN journal
02775387
Volume
16
Issue
20
Year of publication
1997
Pages
3681 - 3686
Database
ISI
SICI code
0277-5387(1997)16:20<3681:TPSAXC>2.0.ZU;2-A
Abstract
The reaction of 2,6-diacetylpyridinedihydrazone with lead(II) nitrate gives the complex with metal-ligand stoichiometry equal to 1:1, irresp ective of the molar ratio of starting materials. The complex has been characterized by spectral data (IRI H-1 and C-13 NMR), elemental and X -ray crystal structure analysis. (C) 1997 Elsevier Science Ltd.