X-ray absorption spectra have been measured in total-electron yield mo
de at the aluminum K edge in gibbsite and related compounds. The exper
iments were carried out at the UVSOR storage ring in Okazaki, Japan, w
hich is particularly suitable for these measurements because of its re
latively low intensity which permits the use of a quartz monochromator
without causing radiation damage to the quartz. It is shown that XAFS
spectra of good quality can be obtained.