The morphological differences between porous silicon formed in the dar
k or under illumination have been studied by means of gravimetric meas
urements, transmission electron microscopy, infrared spectroscopy and
cyclic voltammetry, Photoetching has been found to give rise to a comp
lex surface structure, due to the presence of narrower outer silicon f
ibres, which suffer a more severe cracking process upon drying, (C) 19
97 by John Wiley & Sons, Ltd.