M. Brill, THE OUTLOOK FOR EQUIPMENT NECESSARY AND S UFFICIENT FOR SPECTROMETRICINORGANIC ELEMENTAL ANALYSIS AFTER THE YEAR 2000, Metall, 51(7-8), 1997, pp. 411-421
With such a compelling topic it was easier to state the problem than t
o solve it. The pragmatic assessment of spectrometric equipment readil
y available on the market today for elemental analysis for a particula
r application ist no easy task; to plan actual equipment necessary but
also sufficient, for the future is an even more difficult undertaking
for an analytical service continually plagued by cost pressures On th
e strength of the rapid progress in the areas of mechanics, optics, el
ectronics, but above all also of mathematical calculation software, a
rationalisation potential only scarred today will be concluded in the
future. As much as possible the development of new equipment should be
for the benefit of rapid and convenient analytical qualify assurance
with direct measurement of samples; installation and operational costs
, such as minimising the chemicals needed and other consumables, hereb
y play a decisive role. For technical progress to be marketable there
must always be two prerequisites the necessity of an improvement and t
he possibility of its realisation. If this in itself trivial situation
is not critically examined, the requirement of the user can easily be
circumvented, who under certain circumstances is no longer able to re
invest in his proven type of spectrometer for the necessary quality as
surance. Consequently backwards steps can occur if shortwinded self-in
terests of the equipment developers with regard to the use of their pr
oducts are reflected negatively in budgets. In today's view, exaggerat
ed requirements for future complete automation of elemental analysis o
n a wide front still appear to be in the realm of Utopia. Nevertheless
experiments on automation also signal complex methods with high accur
acy which have brought success in this direction within grasp. Also in
the future the analyst will have to ensure great care and presence of
mind when developing exacting methods, even if a more efficient speci
alised instrumental laboratory is available to him. The goal of each d
evelopment in this regard can only be to have available an analytical
service of high quality which is not time consuming. Analytical instru
ment technology will, as before, depend on various proven measurement
principles. As a consequence of this, and in the light of possible fut
ure developments, consideration was given to the established methods:
spark-OES, glow discharge-OES, ICP-OES, AAS, WD-XRF and ED-XRF. It is
to be hoped that the development potential in vested in subsidiary bra
nches of these measurement principles will be used in future in favour
of measurement principles themselves.