Y. Suzuki et al., GRAIN-SIZE CONTROL OF TIAL ALLOY WITH FUL LY LAMELLAR MICROSTRUCTURE USING DISCONTINUOUS COARSENING REACTION, Nippon Kinzoku Gakkaishi, 61(8), 1997, pp. 678-683
Discontinuous coarsening reaction have been used to obtain the microst
ructure of fine-grained lamellae in a Ti-46 mol%Al alloy, which is exp
ected to improve ductility at room temperature. The process mas very s
imple because the structure change was performed only by aging subsequ
ent to quenching. The refinement mechanism was investigated by optical
and scanning electron microscopy. The nuclei of discontinuous coarsen
ing reaction were coarsely spaced lamellae which were generated at gra
in boundaries and inside grains of finely spaced lamellae. The nucleat
ion of coarsely spaced lamellae during aging increased with increasing
cooling rates from the liquid phase and the alpha single phase, When
the aging temperature was below 1473 K, the discontinuous coarsening r
eaction occurred preferentially and the microstructure was refined. Th
e refinement by this process was achieved via the following steps: (1)
nucleation of coarsely spaced lamellae, (2) changing the growth direc
tion and (3) suppression of the grain growth. Thermal stability of the
fine-grained microstructure: obtained by this process was quite high.