IODINE ASSAY IN COW MILK - INDUSTRIAL TREATMENTS AND IODINE CONCENTRATION

Citation
R. Pedriali et al., IODINE ASSAY IN COW MILK - INDUSTRIAL TREATMENTS AND IODINE CONCENTRATION, Annali di chimica, 87(7-8), 1997, pp. 449-456
Citations number
19
Categorie Soggetti
Chemistry Analytical","Environmental Sciences
Journal title
ISSN journal
00034592
Volume
87
Issue
7-8
Year of publication
1997
Pages
449 - 456
Database
ISI
SICI code
0003-4592(1997)87:7-8<449:IAICM->2.0.ZU;2-M
Abstract
A kinetic method of analysis based on the Sandell-Kolthoff catalytic r eaction is used for the determination of the iodine content in cows' m ilk. Before being putting up for sale, cows' milk undergoes several in dustrial treatments: homogenization, pasteurization, ultra high temper ature treatment and progressive skimming. The aim of this paper is to assess the effect of the official sanitary treatment and of various th ermal precesses on milk iodine content. Special care is devoted to sam pling in order to analyze samples deriving from the same initial pool. The analytical method is simple and sensitive. Recovery (92 +/- 3%), repeatability (1.6%) and limit of detection (20 mu g/l) are reported. A calibration curve in logarithmic form is proposed.