Sc. Wu et al., MEASUREMENTS OF THE CHANGES IN MICROSTRUCTURE DURING SUPERPLASTIC DEFORMATION, Journal of materials processing technology, 69(1-3), 1997, pp. 203-207
In this paper, changes in the volume fraction of cavities, in the frac
tal dimension of cavities, in the grain size and aspect ratio (the rat
io of the major axis to the minor axis) of grains and in the dislocati
on density during superplastic deformation have been measured quantita
tively. The experimental results show that the volume fraction of the
cavities, the fractal dimension of the cavities and the dislocation de
nsity increase with increase in the degree of deformation. At the earl
y stage of deformation, the increase in the volume fraction of the cav
ities varies slightly with the increase in strain, but beyond a partic
ular strain, the volume fraction of the cavities increases sharply. Th
e stress state has a considerable influence on the growth rate of the
volume fraction of the cavities: at the same strain, the volume fracti
on of the cavities under the plane equi-tensile stress state is greate
r than that under uniaxial tension. However, the volume fraction of th
e cavities at fracture under the plane equi-tensile stress state is sm
aller than that under the uniaxial tensile-stress state. The grain siz
e after superplastic deformation increases generally, but grain fining
after superplastic deformation is also discovered sometimes, due depe
nding upon the type or commercial state of the metal: of course, it is
related to the stress state in addition. The aspect ratio of the grai
ns tends to the increase with the increase of strain, but it increases
only slowly. (C) 1997 Elsevier Science S.A.