THE DETERMINATION OF TRANS UNSATURATED FATTY-ACIDS IN EDIBLE OILS ANDFATS BY CAPILLARY GAS-LIQUID-CHROMATOGRAPHY

Citation
A. Dieffenbacher et P. Dysseler, THE DETERMINATION OF TRANS UNSATURATED FATTY-ACIDS IN EDIBLE OILS ANDFATS BY CAPILLARY GAS-LIQUID-CHROMATOGRAPHY, Pure and applied chemistry, 69(8), 1997, pp. 1829-1837
Citations number
3
Categorie Soggetti
Chemistry
Journal title
ISSN journal
00334545
Volume
69
Issue
8
Year of publication
1997
Pages
1829 - 1837
Database
ISI
SICI code
0033-4545(1997)69:8<1829:TDOTUF>2.0.ZU;2-0
Abstract
Collaborative studies on the application of capillary gas-liquid chrom atography for the determination of trans unsaturated fatty acids are d escribed. The method investigated involves preparation of methyl ester s with methanolic potassium hydroxide followed by analysis of fatty ac id methyl esters by gas-liquid chromatography on polar capillary colum ns. Care has to be taken in selecting working conditions to obtain the best obtainable resolution of signals necessary for reliable identifi cation and determination of trans unsaturated fatty acids.