H. Bluhm et al., STUDY OF THE INFLUENCE OF NATIVE-OXIDE LAYERS ON ATOMIC-FORCE MICROSCOPY IMAGING OF SEMICONDUCTOR SURFACES, Applied physics. A, Solids and surfaces, 59(1), 1994, pp. 23-27
We have investigated the influence of the native oxide layer on semico
nductor surfaces on the imaging properties of the atomic force microsc
ope operated under ambient conditions by using epitaxial In1-xGaxAs la
yers grown by Metal-Organic Chemical Vapour Deposition (MOCVD) on (001
) oriented InP substrates which have been kept under ambient condition
s for two years. The thickness and composition of the native oxide lay
ers were studied with ellipsometry and X-ray photoelectron spectroscop
y, respectively. Subsequently, the sample surfaces were imaged by mean
s of atomic force microscopy operated in air which revealed terrace st
ructures separated by monoatomic steps. The obtained data were compare
d with the surface morphology which can be expected from the MOCVD gro
wth process. The results suggest that an accurate study of semiconduct
or layer growth by atomic force microscopy in air is possible.