K. Takano et al., RELATIONSHIP BETWEEN GROWN-IN DEFECTS AND THERMAL HISTORY DURING CZ SI CRYSTAL-GROWTH, Journal of crystal growth, 180(3-4), 1997, pp. 363-371
An abrupt change of the crystal growth rate at temperatures in the ran
ge 1150-1080 degrees C affects the annihilation or the agglomeration o
f grown-in defects such as flow pattern defects (FPD), crystal origina
ted particles (COP), laser scattering defects (LSTD) and the defects m
easured by an optical precipitate profiler (OPPDs). Moreover, it is de
monstrated that the densities of FPDs and LSTDs correlate with each ot
her, and also with the cooling rate in such a temperature range. These
relationships were investigated by growing several silicon single cry
stals in 10 kinds of hot-zone (HZ) configurations designed by using a
numerical simulation. The cooling rate from 1412 degrees C, the meltin
g point of silicon, to 1150 degrees C does not seem to be so important
for the generation or the annihilation of these defects.