Vt. Volkov et al., FORMATION AND SCANNING ELECTRON-MICROSCOPY INVESTIGATION OF LINBO3 FILMS ON SILICON SUBSTRATES, Integrated ferroelectrics, 9(4), 1995, pp. 261-269
The process of the production of LiNbO3 thin films by sputtering onto
fold silicon substrates followed by heat treatment was investigated. C
omposition, structure and physical properties of the films were invest
igated using light refractive indices, theta - 2 theta X-ray diffracti
on and scanning electron microscopy, capacitance and dielectric consta
nt measurements. The amount of the crystalline phase of the stoichiome
tric composition was found to be about 90%. The refractive index (lamb
da = 632.8 nm) and the dielectric constant of the best samples were as
high as 2.28 and 40, respectively. Insulating properties of this film
structure were studied by SEM using e-beam sample charging. The poten
tial images of the film structure provided evidence that current leaka
ge takes place in the boundary areas between the crystallite and noncr
ystallite phases.