K. Wago et al., LOW-TEMPERATURE MAGNETIC-RESONANCE FORCE DETECTION, Journal of vacuum science & technology. B, Microelectronics and nanometer structures processing, measurement and phenomena, 14(2), 1996, pp. 1197-1201
A low-temperature magnetic resonance force microscope (MRFM) has been
built and a force sensitivity of 8 x 10(-17) N/root Hz has been achiev
ed using a single-crystal silicon cantilever with a Q of 200 000 at 6
K. Nuclear magnetic resonance (NMR) of F-19 was measured via force det
ection in a 1% Nd-doped CaF2 sample mounted on the cantilever. Cyclic
adiabatic inversion of the F-19 nuclear spins was performed using a fr
equency modulated radio frequency field at 100 MHz, resulting in an os
cillatory magnetic force that excited the cantilever vibration. NMR fo
rce signals were measured in the temperature range between 12 and 40 K
. The MRFM technique was also used to measure some basic NMR propertie
s such as spin-lattice relaxation time. (C) 1996 American Vacuum Socie
ty.