Xb. Hu et al., THE FORMATION MECHANISMS OF DISLOCATIONS AND NEGATIVE CRYSTALS IN LIB3O5 SINGLE-CRYSTALS, Journal of crystal growth, 163(3), 1996, pp. 266-271
Dislocations and negative crystals in LiB3O5(LBO) single crystals were
investigated by white-beam synchrotron radiation topography (WBSRT) a
nd birefringence image. The WBSRT revealed that the grown-in dislocati
ons are mainly pure screw or edge types with the Burgers vectors in th
e low index directions on the (010) lattice plane. Based on the struct
ure analysis, the cause of the formation of dislocations can be interp
reted in terms of the loose packing of B-O rings on the (010) lattice
plane. In addition, the negative crystals, which were observed by the
birefringence image, tend to present at regular shapes which are simil
ar to that of the host crystal, It is proposed that the negative cryst
als result from the formation of liquid parent inclusions and the foll
owing inward growth.