REFINEMENT OF -4-(TRICYCLO[3.3.1.1(3,7)]DEC-1-YL)-1,3,5-TRIAZINE AT 3DIFFERENT TEMPERATURES USING IMAGE-PLATE DATA

The structure of ino-6-(4-methyl-1-piperazinyl)-4-(tricyclo[3.3.1.1 (3 ,7)]dec-1-yl)-1,3,5-triazine was refined using data collected at three different temperatures [room temperature (293 K), 150 K and 85 K] wit h the use of an image-plate scanner in an attempt to study the effect of temperature on the disorder of the adamantyl group. It is demonstra ted that the data collected with the rotation method and an image-plat e scanner are of a high enough quality to be used for the refinement o f small-molecule structures.