Ya. Lisovskii et al., THE STRUCTURE AND MAGNETIC-PROPERTIES OF CO-CR THIN-FILMS FOR PERPENDICULAR RECORDING, Materials chemistry and physics, 44(3), 1996, pp. 239-244
X-ray analysis, Auger electron spectroscopy (AES), transmission electr
on microscopy (TEM), and high-voltage transmission electron microscopy
(HVTEM) are employed to study the fine structure of a Co-Cr work laye
r of a multilayer thin-film system for high-density perpendicular magn
etic recording. Variations in structure and magnetic properties versus
processing parameters are shown. Thin films prepared with optimal tec
hnology have a columnar structure with a strong axial texture (c-axis
is normal to the film surface) with dispersion up to approximate to 1.
5 around the surface normal and in the perpendicular direction. HVTEM
studies show that similarly oriented grains are gathered, in the micro
structure, into clusters. Precipitates, identified with a micro-microd
iffiaction method, are found as being of a different character on inte
rnal low-angle grain boundaries of clusters than on external ones, whi
ch are classified as random grain boundaries. The existence of homogen
eous magnetic volumes distinguishable from grain size is brought out u
sing Lorentz microscopy. A correlation between coercivity and cluster
size is found.