The production of consistent high purity materials is critical for imp
rovement in performance and sensitivity of II-VI photovoltaic and phot
oconductive devices. Information regarding the energy band structure a
nd impurity or defect levels present in the material is essential to u
nderstand and enhance the performance of current detectors along with
the development of future novel devices. Secondary ion mass spectromet
ry (SIMS) is capable of providing information of purity, junction dept
hs, dopant distribution, and stoichiometry in the material. SIMS techn
iques can achieve high detection sensitivities in very small analytica
l volumes and for a wide range of elements (almost the entire periodic
table). SIMS analysis also provides unique capabilities for localizing
atomic distribution in two and three dimensions. Ion images can be ob
tained by registering the positions of mass selected ions formed in th
e sputtering process. The combination of excellent detection sensitivi
ty, high mass resolution, depth profiling capability, and high resolut
ion image acquisition on a wide spectrum of elements by a SIMS instrum
ent is not matched by any other instrumentation technique.