DIFFERENTIAL-PULSE POLAROGRAPHIC-DETERMINATION OF SALICYLALDEHYDE AS ITS GIRARD-P DERIVATIVE

Authors
LOPEZ LJM MOCHON MC SANCHEZ JCJ PEREZ AG
Citation
Ljm. Lopez et al., DIFFERENTIAL-PULSE POLAROGRAPHIC-DETERMINATION OF SALICYLALDEHYDE AS ITS GIRARD-P DERIVATIVE, Mikrochimica acta, 124(3-4), 1996, pp. 187-194
Citations number
26
Categorie Soggetti
Chemistry Analytical
Journal title
Mikrochimica acta → ACNP
ISSN journal
00263672
Volume
124
Issue
3-4
Year of publication
1996
Pages
187 - 194
Database
ISI
SICI code
0026-3672(1996)124:3-4<187:DPOSAI>2.0.ZU;2-2
Abstract
A method for the determination of salicylaldehyde (2 x 10(-6)-10(-4) M ) by differential-pulse polarography, based on the in situ formation o f its Girard-P derivative in aqueous solution at pH 2.5, is proposed. The relative standard deviation was 1.5% (ten determinations of 4 x 10 (-5) M level). The applicability of this method was checked in synthet ic samples containing salicyl alcohol, o-aminophenol, 2-methylphenol, salicylic acid and 4-aminobenzoic acid.