B. Steiner et al., RESIDUAL DISORDER IN LOW-PRESSURE, LOW THERMAL-GRADIENT LIQUID ENCAPSULATED CZOCHRALSKI GALLIUM-ARSENIDE OBSERVED IN HIGH-RESOLUTION SYNCHROTRON DIFFRACTION IMAGING, Journal of crystal growth, 169(1), 1996, pp. 1-12
High resolution synchrotron X-radiation diffraction images of low ther
mal gradient, low pressure, liquid encapsulated Czochralski (LEG) sili
con-doped gallium arsenide display a degree of crystalline order that
is far higher than that found in undoped conventional LEC material. No
distinct Volume irregularity is observed in one crystal where it is u
nstrained. Only a set of surface-treatment-related dislocations is pro
minent in a second. A third crystal exhibits two distinct sets of quas
i periodic dislocations, which have been analyzed in detail. The resul
ts support a model previously proposed for the evolution of disorder i
n gallium arsenide and suggest the role that silicon plays in its cont
rol.