S. Geremia et al., A METHOD OF ALIGNMENT OF A 4-CIRCLE DIFFRACTOMETER USING A SMALL COLLIMATOR IN THE CENTER OF THE EULERIAN CRADLE, Journal of applied crystallography, 27, 1994, pp. 1061-1063
A procedure is described that uses a small collimator in the center of
the Eulerian cradle for the alignment of the incident beam, the zero
positions of the circles and the collimators of a four-circle diffract
ometer. The method is applicable also with a large initial misalignmen
t of the diffractometer. The results obtained indicate a high reproduc
ibility of the zero-position values, with deviations of the order of t
he step accuracy of the angle setting.